ID21 - X-ray Microscopy Beamline

Contacts

Tel: +33 (0) 476 88 +ext

Fax: +33 (0) 476 88 2542

Marine Cotte 2127
Scientist in charge

Murielle Salome 2607
Beamline operation manager

Synopsis

ID21 will restart in 2020 focusing its activity on the in-vacuum scanning X-ray microscope (SXM). This microscope should offer a beam of ~ 0.3µm Vx0.7µm H for 2D µXRF (elemental maps) and µXANES (chemical speciation in 0D, 1D and 2D) in the energy range 2-9 keV. An additional nanoscope is currently under design, that should be commissionned in 2010.

Status: open

Disciplines

Medicine
Cultural Heritage
Environmental Sciences
Earth and Planetary Sciences
Materials and Engineering
Physics
Life Sciences
Chemistry

Applications

Cultural Heritage (e.g. paintings, ceramics, glasses)
Biology (e.g. nano-toxicology, pathology, metallobiology, health)
Geochemistry (e.g. basaltic glasses, sediments)
Environmental sciences (e.g. soils, phytoremediation, pollution)
Materials (e.g. nano-materials, energy)

Techniques

MicroXANES - micro X-ray absorption near-edge structure
MicroXRF - micro X-ray fluorescence
XANES - X-ray absorption near-edge structure
XAS - X-ray absorption spectroscopy
XRF - X-ray fluorescence

Energy range

2.1 - 9.2 keV

Beam size

Minimum (H x V) : 0.7 x 0.3 µm²
Maximum (H x V) : 2.0 x 2.0 mm²

Sample environments

SXM: In vacuum operation; Cryo-stage; Wet cell

Detectors

SXM end-station (2.1 - 9.2 keV, 0.7 x 3 µm² to 2 x 2 mm [hxv]): regularly used Si photodides; SGX 100mm² SiriusSD silicon drift diode.

Technical details

M. Cotte, E. Pouyet, M. Salomé, C. Rivard, W. De Nolf, H. Castillo-Michel, T. Fabris, L. Monico, K. Janssens, T. Wang, P. Sciau, L. Verger, L. Cormier, O. Dargaud, E. Brun, D. Bugnazet, B. Fayard, B. Hesse, A. E. Pradas del Real, G. Veronesi, J. Langlois, N. Balcar, Y. Vandenberghe, V. A. Solé, J. Kieffer, R. Barrett, C. Cohen, C. Cornu, R. Baker, E. Gagliardini, E. Papillon and J. Susini, "The ID21 X-ray and infrared microscopy beamline at the ESRF: status and recent applications to artistic materials." Journal of Analytical Atomic Spectrometry (2017). http://pubs.rsc.org/-/content/articlehtml/2016/ja/c6ja00356g

M. Salomé, M. Cotte, R. Baker, R. Barrett, N. Benseny-Cases, G. Berruyer, D. Bugnazet, H. Castillo-Michel, C. Cornu, B. Fayard, E. Gagliardini, R. Hino, J. Morse, E. Papillon, E. Pouyet, C. Rivard, V. A. Solé, J. Susini and G. Veronesi, "The ID21 Scanning X-ray Microscope at ESRF", Journal of Physics: Conference Series, 425, 182004 (2013). http://dx.doi.org/10.1088/1742-6596/425/18/182004

VIEW ALL SPOTLIGHTS

12-06-2019

Inflammation increases gadolinium retention in the brain after administration of a linear gadolinium-based contrast agent

03-01-2019

Tracing titanium dioxide nanoparticles in the environment

05-04-2018

Revealing Old Masters pigment grades by synchrotron X-ray diffraction

NEWS FROM ID21

VIEW ALL NEWS

15-05-2020

Researchers find the key to preserving The Scream

01-05-2020

Out of the blue: X-rays shed light on on ultramarine blue in masterpieces

21-11-2019

How cadmium in algae alters the carbon cycle

Synopsis

Status: open

Disciplines

Medicine
Cultural Heritage
Environmental Sciences
Earth and Planetary Sciences
Materials and Engineering
Physics
Life Sciences
Chemistry

Applications

Cultural Heritage (e.g. paintings, ceramics, glasses)
Biology (e.g. nano-toxicology, pathology, metallobiology, health)
Geochemistry (e.g. basaltic glasses, sediments)
Environmental sciences (e.g. soils, phytoremediation, pollution)
Materials (e.g. nano-materials, energy)

Techniques

MicroXANES - micro X-ray absorption near-edge structure
MicroXRF - micro X-ray fluorescence
XANES - X-ray absorption near-edge structure
XAS - X-ray absorption spectroscopy
XRF - X-ray fluorescence

Energy range

2.1 - 9.2 keV

Beam size

Minimum (H x V) : 0.7 x 0.3 µm²
Maximum (H x V) : 2.0 x 2.0 mm²

Sample environments

SXM: In vacuum operation; Cryo-stage; Wet cell

Detectors

SXM end-station (2.1 - 9.2 keV, 0.7 x 3 µm² to 2 x 2 mm [hxv]): regularly used Si photodides; SGX 100mm² SiriusSD silicon drift diode.

Technical details

Latest publications

View all publications

Antioxidant effect of phenolic compounds (PC) at different concentrations in IEC-6 cells: A spectroscopic analysis

Barraza-Garza G., Pérez-León J.A., Castillo-Michel H., de la Rosa L.A., Martínez-Martínez A., Cotte M., Alvarez-Parrilla E.,
Spectrochimica Acta A 227, 117570-1-117570-8 (2020)

Calcium redistribution contributes to the hard-to-cook phenotype and increases PHA-L lectin thermal stability in common bean low phytic acid 1 mutant seeds

Cominelli E., Galimberti M., Pongrac P., Landoni M., Losa A., Paolo D., Daminati M.G., Bollini R., Cichy K.A., Vogel-Mikus K., Sparvoli F.,
Food Chemistry 321, 126680-1-126680-10 (2020)

Non‐spherical pearl layers in the Polynesian ‘black‐lipped’ Pinctada margaritifera : The non‐nacreous deposits compared to microstructure of the shell growing edge

Cuif J.P., Dauphin Y., Luquet G., Belhadj O., Rouzière S., Salomé M., Cotte M., Somogyi A., Medjoubi K., Lo C., Saulnier D.,
Aquaculture Research 51, 506-522 (2020)

Inside black pearls

Dauphin Y., Belhadj O., Bellot-Gurlet L., Cotte M., Lo C., Medjoubi K., Somogyi A., Salomé M., Cuif J.P.,
Materials Characterization 163, 110276-1-110276-13 (2020)

Nicotianamine synthase 2 is required for symbiotic nitrogen fixation in medicago truncatula nodules

Escudero V., Abreu I., del Sastre E., Tejada-Jimenez M., Larue C., Novoa-Aponte L., Castillo-Gonzalez J., Wen J.Q., Mysore K.S., Abadia J., Argüello J.M., Castillo-Michel H., Alvarez-Fernandez A., Imperial J., Gonzalez-Guerrero M.,
Frontiers in Plant Science 10, 1780-1-1780-14 (2020)

Probing the chemistry of CdS paints in The Scream by in situ noninvasive spectroscopies and synchrotron radiation x-ray techniques

Monico L., Cartechini L., Rosi F., Chieli A., Grazia C., De Meyer S., Nuyts G., Vanmeert F., Janssens K., Cotte M., De Nolf W., Falkenberg G., Sandu I.C.A., Storevik Tveit E., Mass J., Pereira de Freitas R., Romani A., Miliani C.,
Science Advances 6, eaay3514-1-eaay3514-12 (2020)